This article studied chromium azure CAS-CTMAB the spectrophotometric method determination determination steel slag EDTA- alkaline solution to soak takes in the fluid the aluminum content, Al3+ and chromium azure S produces the red dual complex compound in the low-acid solution, biggest absorption wave length λmax=560nm, mole of absorption coefficient κ=×104L•mol-1• time Al3+ and chromium azure S, if joins includes the long carbon chain organic surface active agent, like bromination hexadecyl trimethyl ammonium (CTMAB).Then may form three Yuan complex compounds, its biggest absorption wave length to the long wave traverse (red shift), the mole of absorption coefficient increases 2~3 times, the determination sensitivity remarkable hexadecyl trimethyl bromination amine (CTMAB) increases the sensitive medicinal preparation as the aluminum and the chromium azure S color reaction, in an ethanoic acid sodium acetate cushion medium, when pH =, this system has the biggest absorption peak in 615 nm, the aluminum content conforms to Lang in μg/50ml scope Bo a birr law, correlation coefficient r=, regression equation y=, the method picks out limits is , apparent mole of extinction coefficient ε600 = ×105L•mol- 1• method does not need to use the expensive equipment, the coloration is keen, the stability is good, the operation is simple, can obtain the good accuracy and the accuracy.
一、毕业论文(设计)资料按以下顺序排列: (一)封面。包括论文题目、指导教师、学生姓名、学号、院(系)、专业、毕业时间等内容。论文封面由学校统一印制。 (二)中、外文摘要(包括关键词)。外文论文(设计)的中文摘要放在英文摘要后面编排。 (三)正文。 (四)注释。 (五)附录(附图)。 (六)参考文献。 (七)致谢。 二、毕业论文的打印与装订 除要检验学生书写规范的专业外,毕业论文(设计)须用计算机打印,一律采用A4纸。 (一)页面设置 毕业论文(设计)要求纵向打印,页边距的要求为: 上(T): cm 下(B): cm 左(L):2 cm 右(R):2 cm 装订线(T): cm 装订线位置(T):左 其余采取系统默认设置。 (二)排式与用字 文字图形一律从左至右横写横排。 文字一律通栏编辑。 论文采用宋体,字迹清楚整齐,除特殊需要,一般不使用繁体字。 (三)段落设置 采用多倍行距,行距设置值为。 其余采取系统默认设置。 (四)页眉、页脚设置 论文题目(不包括副题目)居中,采用五号宋体字。 页脚需设置页码,页码采用五号黑体字,加粗,居中放置,格式如:1,2,3……页。 三、毕业论文(设计)撰写的内容与要求 (一)封面 1、封面。 纸质封面由学校统一印制。不编排页码。 2、封一(中文摘要) 中文摘要:“中文摘要”四字在第一行居中位置,使用小二号黑体字,加粗。内容使用小四号宋体字。起行空两格,回行顶格。中文摘要一般不超过250—300字。 关键词:接中文摘要打印,“关键词”三字空两格,后加冒号与关键词隔开,各关键词之间用逗号隔开。关键词一般在3—8个之间。 3、封二(外文摘要) 外文摘要:“外文摘要”英文单词在第一行居中位置,使用小二号黑体字,加粗。内容使用小四号宋体字。起行空两格,回行顶格。外文摘要一般不超过250个实词。 关键词:接外文摘要打印,“关键词”英文单词空两格,后加冒号与关键词隔开,各关键词之间用逗号隔开。外文关键词应与中文关键词相对应。 (二)正文 正文一般使用小四号宋体字,重点文句加粗。 1、标题层次。 毕业论文的全部标题层次应整齐清晰,相同的层次应采用统一的表示体例,正文中各级标题下的内容应同各自的标题对应,不应有与标题无关的内容。 各层标题均单独占行。第一级标题居中放置;第二、三、四等级标题序数顶格放置,后空一格接标题内容,末尾不加标点。 标题序数采用1.、2.……、……、…………的层次。正文中对总项包括的分项采用一、二、……(一)、(二)……1、2……(1)、(2)……①②……的层次,括号后不再加其他标点。 2、量和单位。各种计量单位一律采用国家标准GB3100—GB3102-93。非物理量的单位可用汉字与符号构成组合形式的单位。 3、标点符号。标点符号应按照国家新闻出版署公布的“标点符号使用方法”的统一规定正确使用,忌误用和含糊混乱。 4、外文字母。外文字母采用我国规定和国际通用的有关标准写法。要分清正斜体、大小写和上下脚码。 5、名词、名称。科学技术名词术语采用全国自然科学技术名词审定委员会公布的规范词或国家标准、部标准中规定的名称,尚未统一规定或叫法有争议的名称术语,可采用惯用的名称。 6、数字。文中的数字,除部分结构层次序数和词、词组、惯用语、缩略语、具有修辞色彩语句中作为词素的数字必须使用汉字外,应当使用阿拉伯数码,同一文中,数字表示方法应前后一致。 7、公式。公式一般居中放置;有编号的公式顶格放置,编号需加圆括号标在公式右边,公式与编号之间不加虚线。 公式下有说明时,应在顶格处标明“注:”。 较长公式的转行应在加、减、乘、除等符号处。 8、表格和插图。 (1)表格。每个表格应有自己的表序和表题。表内内容应对齐,表内数字、文字连续重复时不可使用“同上”等字样或符号代替。表内有整段文字时,起行处空一格,回行顶格,最后不用标点符号。 (2)插图。每幅图应有自己的图序和图题。一般要求采用计算机制图。 文中图表需在表的上方、图的下方排印表号、表名、表注或图号、图名、图注。 (三)注释注释采用页末注(将注文放在加注页的页脚)或篇末注(将全部注文集中在文章末尾),不可行中加注。注释编号选用带圈阿拉伯数字,注文使用小五号宋体字。以下为引用各类文献注释格式:专著:注释编号.作者.专著.书名[M].出版社,出版年.起止页码 期刊:注释编号.作者.期刊.题名[J].刊名,出版年(卷、期):起止页码 论文集:注释编号.作者.论文名称: 论文集名[C].出版地:出版社,出版年度.起止页码 学位论文:注释编号 .作者.题名[D].保存地点:保存单位,写作年度. 专利文献:注释编号.专利所有者.题名[P].专利国别:专利号, 出版日期光盘:注释编号.责任者.电子文献题名[电子文献及载体类型标识],出版年(光盘序号) 互联网:注释编号.责任者.文献题名.电子文献网址.访问时间(年-月-日)文献作者3名以内的全部列出;3名以上则列出前3名,后加“等”(英文加“etc"”) (四)附录 “附录”两字在第一行居中位置,使用小二号黑体字,加粗。 附录项目名称使用四号黑体字,加粗,居左顶格放置。另起一行空两格,使用小四号宋体字标注附录序号和题名,编排样式可参照正文。 (五)参考文献 参考文献一律放在文后,其书写格式应根据GB3469-83《文献类型与文献载体代码》规定,以单字母方式标识:M专著,C论文集,N报纸文章,J期刊文章,D学位论文,R研究报告,S标准,P专利;对于专著、论文集中的析出文献采用单字母“A”标识,其他未说明的文献类型,采用单字母“Z”标识。 “参考文献”四字居中放置,使用小二号黑体字,加粗。 内容使用小四号宋体字,居左,空两格放置。具体结构格式与标注方法同注释中交代引文出处的注文格式。
毕业论文的Abstract简单说就是毕业论文的英文摘要,先把中文摘要写好,然后翻译成英文就可以了。摘要也就是内容提要,是论文中不可缺少的一部分。论文摘要是一篇具有独立性的短文,有其特别的地方。它是建立在对论文进行总结的基础之上,用简单、明确、易懂、精辟的语言对全文内容加以概括,留主干去枝叶,提取论文的主要信息。作者的观点、论文的主要内容、研究成果、独到的见解,这些都应该在摘要中体现出来。好的摘要便于索引与查找,易于收录到大型资料库中并为他人提供信息。因此摘要在资料交流方面承担着至关重要的作用。书写摘要的基本规范和原则:1、论文摘要分为中文摘要和外文(一般为英文)摘要。摘要在篇幅方面的限定,不同的学校和机构有不同的要求,通常中文摘要不超过300字,英文摘要不超过250个实词,中英文摘要应一致。毕业论文摘要可适当增加篇幅。2、多向指导教师请教,并根据提供的意见及时修改,以期达到更高水平。3、摘要是完整的短文,具有独立性,可以单独使用。即使不看论文全文的内容,仍然可以理解论文的主要内容、作者的新观点和想法、课题所要实现的目的、采取的方法、研究的结果与结论。4、叙述完整,突出逻辑性,短文结构要合理。5、要求文字简明扼要,不容赘言,提取重要内容,不含前言、背景等细节部分,去掉旧结论、原始数据,不加评论和注释。采用直接表述的方法,删除不必要的文学修饰。摘要中不应包括作者将来的计划以及与此课题无关的内容,做到用最少的文字提供最大的信息量。6、摘要中不使用特殊字符,也不使用图表和化学结构式,以及由特殊字符组成的数学表达式,不列举例证。
Hot Deformation Behavior of metal an important aspect of research is to study the metal in the process of hot deformation behavior of the flow stress, as well as changes in the law of the mechanical properties of the macro-response behavior is the flow stress. According to the theory of deformation, the flow stress of metal materials in a one-way refers to the deformation conditions sufficient to achieve plastic deformation of the stress intensity. Metals and alloys in the plastic working process, the flow stress determined the deformation of the size of equipment needed to load and the size of the required energy consumption. Generally speaking, the impact of the metal flow stress factors in general can be divided into internal factors and external factors. The main external factors, including deformation temperature, strain rate and strain (deformation), they are internal factors of the flow stress of metallic materials. Deformation temperature on the impact of flow stress as follows: flow stress with deformation temperature lower, but reduced somewhat different, that is, the higher strain rate, with the increase in deformation temperature, flow stress gradient reduced more Great. Strain rate on the impact of flow stress: the higher the strain rate, the greater the value of flow stress, and increase the flow stress with temperature changes, temperature, the higher the lower the rate of increase. The rate of increase of flow stress is not maintained at a fixed value, but as the strain rate changes. Internal factors include the chemical composition of metals, metal the microstructure changes such as dynamic recovery and dynamic recrystallization, such as work hardening. High-temperature mechanical deformation of metallic materials from high temperature creep behavior of metals on the basis of developed. Metals and alloys the existence of thermal processing thermal activation process, the strain rate thermal activation process control. Deformation under different conditions using different expressions, but also related to thermal activation, the dislocation movement, such as the micro-mechanism. This paper AZ31 magnesium alloy sheet for the study, the RG-based microcomputer-controlled universal testing machine, metallographic microscope and scanning electron microscopy tools, research and analysis of magnesium alloy at different temperatures forming performance, flow stress and microstructure changes in the law. The following conclusions: 1. Extrusion, cross-rolling, cold-rolled, hot-rolled, as well as the level of casting AZ31 magnesium alloy sheet metal microstructure is equiaxed structure, the grain size of 5 ~ 25μm; 2. Extrusion of magnesium alloy sheet metal grain size is about 5 ~ μm, the strain rate is less than , the deformation temperature is higher than 150 ℃, the extension rate of greater than 45%, and with the strain rate lower or raise the temperature of the peak flow stress also be reduced accordingly. When the temperature is 425 ℃, then the peak steady-state flow stress is almost equal to the flow stress at the time that the peak stress does not appear, and its value in between 18 ~ 20MPa, and the extension rate of 132%. 3. Cross-rolled sheet metal so that the peak flow stress decreased significantly increased plasticity. (And can reduce or eliminate the anisotropic material to improve the performance of its punch, so that elongation of the material significantly increased for deep-drawing deformation even provided a good internal organization.) At a temperature of 425 ℃, strain rate is less than , the elongation δ> 225%, alloy shows superplasticity. 4. 250 ~ 425 ℃ temperature range, semi-continuous casting + annealing cold-rolled sheet before and after the stress - strain curve changes little elongation δ are greater than 65%. Cold-rolled sheet can be used directly in temperatures greater than 250 ℃ forming thermal processing. 5. At a high temperature to soften and as a result of the role of dynamic recrystallization results of horizontal continuous casting + anisotropic cold-rolled sheet has been significantly improved. At 250 ℃ when the sheet are an extension of the rate of 118 percent, the smallest anisotropy alloys. 6. At a temperature less than 220 ℃, the fracture morphology of the main axis for large and small dimples, such as composition, surface tear edge clarity, and depth of dimples smaller size; When the temperature is greater than 240 ℃ when the equiaxed the edge of dimples appear fine grains, the occurrence of a fracture. Magnesium alloy at high temperature phase of the basic fracture along fracture, with the strain rate increased, the fracture mode transformed to the ductile fracture trend. AZ31 magnesium alloy in the plastic deformation occurred during the dynamic recrystallization and grain growth.
Title: In the ointment of diosgenin and Smilax saponin Identification of Erdong GaoAbstract: Objective: Cream of the Erdong in the chemical composition of a preliminary study. Method: macroporous resin adsorption chromatography, column chromatography and gel column chromatography glucan combination of methods to separate. Results: Plaster from the winter of chloroform isolated two compounds, through physical and chemical properties and spectral analysis of its structure identified as diosgenin and Smilax saponin. Conclusion: explored and the Isolation method is simple and easy. Key words: Erdong Gao,Erdong cream, diosgenin saponin, Smilax saponin, Isolation太专业了。的确让人头大。终于棒你翻译出来了!二冬膏我查了下,一般只有拼音名的,所以这里也沿用。
In this paper, the CAS-CTMAB chromazurol Determination Determination of EDTA-alkali slag leaching liquid solution of aluminum content, Al3 + and chromazurol S in the weak acid to form a red solution of the binary complex, the largest absorption wavelength λmax = 560nm, the molar absorption coefficient κ = × 104L • mol-1 • cm-1. Al3 + and S chromazurol reactions, the inclusion of long carbon chain containing organic surfactants such as cetyl trimethylammonium bromide (CTMAB). Ternary complex can be formed, and its maximum absorption wavelength to the long-wave direction (red shift), the molar absorption coefficient increased 2 ~ 3 times the determination of the sensitivity significantly. Select CTAB amine (CTMAB) chromazurol as aluminum and the color reaction of S-sensitizing agent, in a sodium acetate buffer solution, when pH = , the system in the 615 nm maximum absorption peak, aluminum content in the range of ~ μg/50ml in line with the Lambert-Beer's law, the correlation coefficient r = , regression equation y = , the detection limit is 0. 005mg / L, the apparent molar absorptivity ε600 = × 105L • mol-1 • cm-1. This method does not require the use of expensive equipment, the color sensitivity, good stability and easy to operate, to get a better precision and accuracy.
Topic: In two winter paste Chinese yam soap glucoside Yuan Heba qia soap glucoside Yuan separation appraisal abstract: Goal: Conducts the preliminary study to in two winter paste chemical : Uses the method which the pocket resin adsorption chromatography, the silica gel column chromatographic analysis law as well as the glucosan gelatin column chromatographic analysis unifies to carry on the : The separation obtains two compound from two winter paste chloroform level, through physics and chemistry nature and spectrum analysis its structure appraisal for Chinese yam soap glucoside Yuan Heba qia soap glucoside : Tried to find out separation method simple, easy line.
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